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Photocatalysts: Synthesis and Characterization Methods offers a systematic overview of synthesis and characterization of novel and efficient photocatalysts. The book explores the fundamentals of synthesis and characterization of photocatalysts using sophisticated instrumentation techniques for novel energy and environmental related applications. It focuses on synthesis methods, nanostructure control, activity enhancement strategies for various applications, and perspectives of nanostructure materials. Part I of the book covers current synthesis methods whereas Part II provides an overview of spectroscopic, physicochemical and electrochemical characterization methods. The book offers guidelines for designing novel photocatalysts with low cost and high efficiency to meet the demands of the energy and environment related researchers and industries.